5-氨基-2,3,3-三甲基-3H-吲哚合成路线 （共 5 条）
反应条件
1: With hydrogenchloride; SnCl2·2H2O in water
2 h; Reflux;
2: With sodium hydrogencarbonate in water
参考文献
LABORATOIRES SYNTH-INNOVE
Patent: US2012/45851 A1, 2012 ;
Location in patent: Page/Page column 14; 18 ;
反应条件
trifluoroacetic acid; palladium monocarbide in methanol; dichloromethane; water
参考文献
DAKO DENMARK A/S
Patent: US2011/230664 A1, 2011 ;
反应条件
1: sodium nitrate; sulfuric acid / 1 h / 0 - 5 °C
2: hydrogenchloride; SnCl2·2H2O / water / 2 h / Reflux
View Scheme
参考文献
LABORATOIRES SYNTH-INNOVE
Patent: US2012/45851 A1, 2012 ;
反应条件
in ethanol
1.5 h; Heating;
参考文献
Lyubich, M. S.; Isaev, Sh. G.; Al'perovich, M. A.; Shpileva, I. S.; Arshava, B. M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 9 p. 976 - 977
Khimiya Geterotsiklicheskikh Soedinenii, 1984 , vol. 20, # 9 p. 1198 - 1199
反应条件
1: 82 percent / ethanol / 0.5 h / 0 - 5 °C
2: 70 percent / ethanol / 2 h / Heating
View Scheme
参考文献
Lyubich, M. S.; Isaev, Sh. G.; Al'perovich, M. A.; Shpileva, I. S.; Arshava, B. M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 9 p. 976 - 977
Khimiya Geterotsiklicheskikh Soedinenii, 1984 , vol. 20, # 9 p. 1198 - 1199
