暂无反应条件数据

暂无反应条件数据

N-bromosuccinmide; triethylamine in dichloromethane T=20°C; Hunsdiecker reaction; 0.0833333 h;

methanol; N-benzyl-trimethylammonium hydroxide in benzene 72 h; Ambient temperature;

1: carbon tetrabromide; triphenylphosphine / dichloromethane / 1.25 h / 0 °C / |Schlenk technique; |Inert atmosphere 2: N-benzyl-N,N,N-triethylammonium chloride; potassium hydroxide / water; dichloromethane / 0 °C / |Schlenk technique; |Inert atmosphere View Scheme

diethyl ether

N-bromosuccinmide; silver nitrate Inert atmosphere;