in ClSO2F (sulfuryl chloride fluoride) inside the drybox; (XeOTeF5)(Sb(OTeF5)6) and CBr4 loaded into vessel at -120°C; removed cold from drybox; placed in a -78°C bath; SO2ClF condensed under static vac.; warmed over period for several hs toabout -50°C; solvent and other volatiles removed under vac. between -78 and 0°C; monitored by NMR spectroscopy and Raman spectroscopy;
参考文献
Journal of the American Chemical Society, , vol. 126, # 17 p. 5533 - 5548
