反应条件
perchloric acid in perchloric acid
very slow addn. of soln. of nitrite (contg. excess of 30percent H2O2) to mixt. of 30percent H2O2 and 70percent HClO4 (-20°C, stirring); simultaneus addn. of 70percent HClO4 to maintain equimolar ratio of NaNO2:HClO4; not isolated, detd. by UV/VIS spectroscopy;
参考文献
Miyamoto, Sayuri; Ronsein, Graziella E.; Correa, Thais C.; Martinez, Glaucia R.; Medeiros, Marisa H. G.; Di Mascio, Paolo
Dalton Transactions, 2009 , # 29 p. 5720 - 5729