ALPHA-溴-4-硝基-O-甲酚合成路线 (共 7 条)
反应条件
hydrogen bromide; acetic acid T=70 - 80°C;
参考文献
Chemische Berichte, , vol. 39, p. 3174
反应条件
1: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / acetonitrile / 2 h / 90 °C / |Inert atmosphere 2: dihydrogen peroxide; water / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 19, # 27 p. 9050 - 9058
反应条件
1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 48 h / 85 °C / |Inert atmosphere 2: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / acetonitrile / 2 h / 90 °C / |Inert atmosphere 3: dihydrogen peroxide; water / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 19, # 27 p. 9050 - 9058
反应条件
water; dihydrogen peroxide T=20°C; Kinetics;
参考文献
Chemistry - A European Journal, , vol. 19, # 27 p. 9050 - 9058
参考文献
Jeong, Kyu-Sung; Hahn, Kyu-Myoung; Cho, Young Lag
Tetrahedron Letters, 1998 , vol. 39, # 22 p. 3779 - 3782
反应条件
1: in dichloromethane; cyclohexane 4.5 h; 2: With boron trifluoride diethyl etherate in cyclohexane; water-d2 3: With water; sodium hydrogencarbonate in dichloromethane; cyclohexane 1 h;
参考文献
WO2007/106546 A2, ;
Page/Page column 12-13 ;
反应条件
boron trifluoride-diethyl ether complex in dichloromethane; cyclohexane