2-苯基-1,3-二恶烷合成路线 （共 72 条）
反应条件
in acetonitrile
T=62°C; P=7500600 Torr; 24 h;
参考文献
Kotsuki, Hiyoshizo; Ichikawa, Yoshikatsu; Nishizawa, Hitoshi
Chemistry Letters, 1988 , p. 673 - 676
反应条件
1: 71 percent / LiAlH4, AlCl3 / diethyl ether / 4 h / Heating
2: triethylamine / 0.25 h / 0 °C
View Scheme
参考文献
Tokoroyama, Takashi; Kusaka, Hisashi
Canadian Journal of Chemistry, 1996 , vol. 74, # 12 p. 2487 - 2502
反应条件
trifluorormethanesulfonic acid in 1,2-dichloro-ethane
T=125°C; 11 h;
参考文献
Fukuzawa, Shin-Ichi; Tsuchimoto, Teruhisa; Hiyama, Tamejiro
Journal of Organic Chemistry, 1997 , vol. 62, # 1 p. 151 - 156
反应条件
hafnium tetrachloride in acetonitrile
T=20°C; Strecker Aminoacid Synthesis; 0.5 h; Inert atmosphere;
参考文献
Zhang, Xue-Lin; Wu, Qin-Pei; Zhang, Qing-Shan
Journal of Chemical Research, 2013 , vol. 37, # 11 p. 690 - 693
反应条件
trimethylsilyl trifluoromethanesulfonate; dimethylsulfide borane complex in dichloromethane
参考文献
Bartels, Birgit; Hunter, Roger
Journal of Organic Chemistry, 1993 , vol. 58, # 24 p. 6756 - 6765
反应条件
carbon monoxide; hydrogen; dicobalt octacarbonyl
T=165°C; P=124116 Torr;
参考文献
Fleming,B.I.; Bolker,H.I.
Canadian Journal of Chemistry, 1976 , vol. 54, p. 685 - 694
反应条件
trifluorormethanesulfonic acid
T=110°C; 7 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Fukuzawa, Shin-Ichi; Tsuchimoto, Teruhisa; Hiyama, Tamejiro
Journal of Organic Chemistry, 1997 , vol. 62, # 1 p. 151 - 156
反应条件
triethylsilane; 1,1,1,3,3,3-hexamethyl-disilazane; iron(II) sulfate in dichloromethane
T=20°C; 36 h;
参考文献
Yang, Bai-Ling; Tian, Shi-Kai
European Journal of Organic Chemistry, 2007 , # 28 p. 4646 - 4650
反应条件
tetra-n-butylammonium tribromide in tetrahydrofuran
T=20°C; 0.08 h;
参考文献
Naik, Sarala; Gopinath, Rangam; Goswami, Mousumi; Patel, Bhisma K.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 11 p. 1670 - 1677
反应条件
in dichloromethane
T=50°C; 0.0833333 h; Microwave irradiationSealed tube;
参考文献
Ramanathan, Mani; Hou, Duen-Ren
Arkivoc, 2013 , vol. 2013, # 3 p. 98 - 108
