in water
addn. of the thiophenol to PbO2 in water, stirring at room temp. for 30 min.; sepn. of the ppt. by filtn., washing with ether and drying, pptn. of the disulfide after concg. the ether washings;
参考文献
Denney, Donald B.; Denney, Dorothy Z.; Liu, Lun-Tsu
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 1 - 8
triethylamine in dichloromethane
T=-50 - 20°C; 20 h; MechanismProduct distribution;
参考文献
Brooke, Gerald M.; Ferguson, J. A. K. Jamie
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2023 - 2026
Platonov, Vyacheslav E.; Bredikhin, Roman A.; Maksimov, Alexander M.; Kireenkov, Victor V.
Journal of Fluorine Chemistry, 2010 , vol. 131, # 1 p. 13 - 16
