1-羟基-2-氧代-1,2,3,4-四氢喹啉合成路线 (共 15 条)
反应条件
titanium(III) chloride in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Kodera; Watanabe; Imada; Murahashi
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 9 p. 2542 - 1549
反应条件
diethylamino-sulfur trifluoride in dichloromethane T=0°C; 0.0833333 h;
参考文献
Kikugawa, Yasuo; Matsumoto, Kazuhiro; Mitsui, Kimiyo; Sakamoto, Takeshi
Journal of the Chemical Society, Chemical Communications, 1992 , # 12 p. 921 - 922
反应条件
sodium tungstate; dihydrogen peroxide
12 h; Ambient temperature;
参考文献
Lion, C.; Hedayatullah, M.; Bauer, P.; Boukou-Poba, J. P.; Charvy, C.; et al.
Bulletin des Societes Chimiques Belges, 1991 , vol. 100, # 8 p. 617 - 621
反应条件
trifluoroacetic acid in dichloromethane
1 h;
参考文献
Cismesia, Megan A.; Ischay, Michael A.; Yoon, Tehshik P.
Synthesis (Germany), 2013 , vol. 45, # 19 art. no. 3889, p. 2699 - 2705
反应条件
hydrogenchloride; hydrogen; Pt/C sulfided in methanol; water
P=2699.3 Torr; 1-2 h;
参考文献
McCord; DuBose; Shafer; Davis
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 3 p. 643 - 646
反应条件
dihydrogen peroxide; sodium tungstate in methanol
50 h; Ambient temperature;
参考文献
Murahashi, Shun-Ichi; Oda, Tetsuya; Sugahara, Toshiaki; Masui, Yoshiyuki
Journal of the Chemical Society, Chemical Communications, 1987 , # 19 p. 1471 - 1472
反应条件
2,6-dimethyl-3,5-diacetyl-1,4-dihydropyridine; camphor-10-sulfonic acid; Ru(bpy)3Cl2*6H2O in tetrahydrofuran; N,N-dimethyl-formamide
16 h; Schlenk techniqueIrradiation; Reagent/catalystConcentration; chemoselective reaction;
参考文献
Cismesia, Megan A.; Ischay, Michael A.; Yoon, Tehshik P.
Synthesis (Germany), 2013 , vol. 45, # 19 art. no. 3889, p. 2699 - 2705
反应条件
palladium diacetate; triethylammonium formate; triphenylphosphine in ethanol; water
0.166667 h; Heating;
参考文献
Kikugawa, Yasuo; Shimada, Masahiro; Matsumoto, Kazuhiro
Heterocycles, 1994 , vol. 37, # 1 p. 293 - 302
反应条件
dihydrogen peroxide; sodium tungstate in methanol
24 h; Ambient temperature;
参考文献
Murahashi, Shun-Ichi; Oda, Tetsuya; Sugahara, Toshiaki; Masui, Yoshiyuki
Journal of Organic Chemistry, 1990 , vol. 55, # 6 p. 1744 - 1749
反应条件
sodium tetrahydroborate; palladium on activated charcoal in methanol; water
0.25 h;
参考文献
Hashimoto; Ishizaki; Shudo; Okamoto
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 11 p. 3891 - 3896