反应条件
in melt
sulphur and selenium were mixed together in molar ratio 70:30, 65:35, 60:40 heated in sealed ampules under reduced pressure (ca. 0.01 kPa) at 770 K for 4 h and quenched at liq. N2 temp.; further products; various product ratio for various conditions;; the resulting amorphous materials were extd. with CS2, after which the solvent was evapd.;;
参考文献
Chivers, Tristram; Laitinen, Risto S.; Schmidt, Kenneth J.
Canadian Journal of Chemistry, 1992 , vol. 70, # 3 p. 719 - 725
