2-(2-苯并噻唑)-1-萘酚合成路线 (共 6 条)
反应条件
1: in toluene
T=90°C;
2: With phosphorus trichoride in toluene
T=60°C; 2 h; Reflux;
参考文献
Kiprof, Paul; Carlson, Jeffrey C.; Anderson, Derrick R.; Nemykin, Victor N.
Dalton Transactions, 2013 , vol. 42, # 42 p. 15120 - 15132
反应条件
benzoic acid in butan-1-ol
T=110°C; 8 h;
参考文献
Yu, Tianzhi; Zhang, Chengcheng; Zhao, Yuling; Chai, Haifang; Fan, Duowang; Ma, Ying; Yao, Shanglei; Li, Wentao
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2013 , vol. 108, p. 274 - 279
反应条件
in 1,4-dioxane
T=100°C; 12 h; Increased pressure;
参考文献
Gracel Display Inc.
Patent: US2010/152455 A1, 2010 ;
Location in patent: Page/Page column 14 ;
反应条件
sodium hydride in N,N-dimethyl-formamide; benzene
T=20°C; Cyclization; oxidation; aromatization; substitution; 168 h;
参考文献
Suma; Asokan
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1999 , vol. 38, # 12 p. 1338 - 1341
参考文献
MERCK PATENT GMBH; KATHIRGAMANATHAN, Poopathy; SURENDRAKUMAR, Sivagnanasumdram; CHAN, Yun Fu
Patent: WO2010/20352 A1, 2010 ;
Location in patent: Page/Page column 64 ;
反应条件
in hexane
T=-80 - 20°C; Kinetics;
参考文献
Graness, A.; Kleinschmidt, J.
Zeitschrift fuer Physikalische Chemie (Leipzig), 1980 , vol. 261, # 6 p. 1152 - 1160