in acetonitrile large excess of a 0.2 M soln. of I2 in acetonitrile at 45°C for 21 days under reduced pressure of N2;; iodine soln. decanted, replaced every 7 days; CuI readily removed by its soly. in acetonitrile;
参考文献
Journal of Solid State Chemistry, , vol. 77, p. 356 - 365
