1-苯基-2-丙烯基-1-酮合成路线 (共 309 条)
反应条件
(2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-pent-2-ene) lithium salt; oxygen; gold(I) chloride in toluene T=90°C; 24 h;
参考文献
Guan, Bingtao; Xing, Dong; Cai, Guixing; Wan, Xiaobin; Yu, Nan; Fang, Zhao; Yang, Liping; Shi, Zhangjie
Journal of the American Chemical Society, 2005 , vol. 127, # 51 p. 18004 - 18005
反应条件
potassium carbonate in benzene 2 h; Reflux;
参考文献
PURDUE RESEARCH FOUNDATION; COLBY, David, A.; RIOFSKI, Mark, V.; HAN, Changho
Patent: WO2012/129384 A2, 2012 ;
Location in patent: Page/Page column 40; 41 ;
反应条件
dihydrogen peroxide in tetrahydrofuran T=0 - 20°C; 0.5 h;
参考文献
Tiwari, Praveen Kumar; Aidhen, Indrapal Singh
Synlett, 2013 , vol. 24, # 14 art. no. ST-2013-B0343-L, p. 1777 - 1780
反应条件
in water T=90 - 95°C; P=750.06 Torr; 0.0266667 h; Irradiation;
参考文献
Cablewski, Teresa; Faux, Alan F.; Strauss, Christopher R.
Journal of Organic Chemistry, 1994 , vol. 59, # 12 p. 3408 - 3412
反应条件
1: in tetrahydrofuran T=0 - 20°C; Weinreb ketone synthesis; Inert atmosphere; 2: With hydrogenchloride in tetrahydrofuran; water pH=2; Inert atmosphere;
参考文献
Uehara, Kazuhiro; Wagner, Christine B.; Vogler, Thomas; Luftmann, Heinrich; Studer, Armido
Angewandte Chemie - International Edition, 2010 , vol. 49, # 17 p. 3073 - 3076
反应条件
platinum (II) chloride; tert-butyl alcohol T=55°C; 16 h; Inert atmosphere;
参考文献
Bhuvaneswari, Sivakolundu; Jeganmohan, Masilamani; Cheng, Chien-Hong
Chemistry - An Asian Journal, 2010 , vol. 5, # 1 p. 141 - 146
反应条件
triethylamine in chloroform T=20°C; 18.0833 h; Inert atmosphere;
参考文献
Chanthamath, Soda; Takaki, Suguru; Shibatomi, Kazutaka; Iwasa, Seiji
Angewandte Chemie - International Edition, 2013 , vol. 52, # 22 p. 5818 - 5821
Angew. Chem., 2013 , vol. 125, # 22 p. 5930 - 5933,4
反应条件
iron tribromide; oxygen in tetrahydrofuran T=-78°C;
参考文献
Corey, E. J.; Walker, Jonathan C.
Journal of the American Chemical Society, 1987 , vol. 109, # 26 p. 8108 - 8109
反应条件
1: vinyl-magnesium bromide With indium(III) chloride in tetrahydrofuran 2: benzoyl chloride With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; 1 h;
参考文献
Lee, Phil Ho; Lee, Sung Wook; Seomoon, Dong
Organic Letters, 2003 , vol. 5, # 26 p. 4963 - 4966
反应条件
water; Hg(OTf)2 in acetonitrile T=20°C; 2 h;
参考文献
Imagawa, Hiroshi; Asai, Yumiko; Takano, Hiroto; Hamagaki, Hitomi; Nishizawa, Mugio
Organic Letters, 2006 , vol. 8, # 3 p. 447 - 450