2-氨基-4,6-二甲基嘧啶合成路线 (共 46 条)
参考文献
E. I. Du Pont de Nemours and Company
Patent: US4238621 A1, 1980 ;
反应条件
selenium; triethylamine in toluene T=150°C; 4 h;
参考文献
Ling, Gang; Chen, Jingzhu; Lu, Shiwei
Journal of Chemical Research - Part S, 2003 , # 7 p. 442 - 444
反应条件
pyridine T=0°C; 2 h; Inert atmosphere;
参考文献
Auxiliadora Dea-Ayuela; Castillo, Encarna; Gonzalez-Alvarez, Marta; Vega, Celeste; Rolon, Miriam; Bolas-Fernandez, Francisco; Borras, Joaquin; Eugenia Gonzalez-Rosende
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 21 p. 7449 - 7456
反应条件
nitrogen oxides; acetic acid
参考文献
Majima
Chemische Berichte, 1908 , vol. 41, p. 185
反应条件
molecular sieve in ethanol 4 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 55, # 7 p. 1070 - 1072
参考文献
Sprague et al.
Journal of the American Chemical Society, 1941 , vol. 63, p. 3028
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Caldwell et al.
Journal of the American Chemical Society, 1941 , vol. 63, p. 2188
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CIBA
Patent: CH230865 , 1938 ;
反应条件
iodine; chlorine in 1,4-dioxane 1.) room temp., 30 min, 2.) 60 deg C, 3 h;
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Yamanaka, Hiroshi
Synthesis, 1984 , # 3 p. 252 - 254
反应条件
in sodium hydroxide; water; acetonitrile
参考文献
E. I. Du Pont de Nemours and Company
Patent: US4546179 A1, 1985 ;
反应条件
1: H2O; CaCO3; chlorine
2: und anschliessenden Hydrolyse mit wss. NaOH
View Scheme
参考文献
Drake et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1602,1603
反应条件
water; chlorine; calcium carbonate
参考文献
Sharp and Dohme Inc.
Patent: US2609372 , 1950 ;
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Drake et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1602,1603