反应条件
HF and NSF3 were condesed in Kel-F reactor at -196°C, allowed toreact at room temp. overnight, SOCl2 added, reacted at room temp. for 2weeks and volatile products were condensed into a NaF scrubber; fractionation through a series of traps at -10, -78, and -196°C in vac., a -78°C trap contained the product, distillation;
参考文献
Thrasher, Joseph S.; Hosmane, Narayan S.; Naurer, Donald E.; Clifford, Alan F.
Inorganic Chemistry, 1982 , vol. 21, p. 2506 - 2508
