solvation of AgNO3 in HF not above 0°C under stirring and introduction of BF3;; precipitation; washing with liquid HF and drying in a stream of N2 (12 hours), later in vacuum (12 hours);;
参考文献
Clifford, A. F.; Kongpricha, S.
Journal of Inorganic and Nuclear Chemistry, 1957 , vol. 5, p. 76 - 78
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Gmelin Handbook: Ag: MVol.B3, 15.9, page 258 - 259
in nitromethane addition of powdered Ag to a solution of HF and BF3 in CH3NO2;;
参考文献
Olah, G.; Quinn, H. W.
Journal of Inorganic and Nuclear Chemistry, 1960 , vol. 14, p. 295 - 296
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Gmelin Handbook: Ag: MVol.B3, 15.9, page 258 - 259
Rezukhina, T. N.; Gorshkova, T. I.; Tsvetkov, A. A.
Russian Journal of Physical Chemistry, 1983 , vol. 57, # 7 p. 1001 - 1004
Zhurnal Fizicheskoi Khimii, 1983 , vol. 57, p. 1651 - 1656