H2O2 in water Ga was reacted with excessive hydrofluoric acid under N2 flow, heated on water-bath, H2O2 was gradually added; product was vaporized until dry on water-bath, residue was heated at 200°C for 2 h under HF flow; X-ray diffraction;
in hydrogen fluoride aq. HF; heating (5 h, 500°C);
参考文献
Opalovskii, A. A.; Gudimovich, T. F.; Kutovaya, L. M.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1979 , vol. 24, p. 604 - 606
Zhurnal Neorganicheskoi Khimii, 1979 , vol. 24, p. 1087 - 1090
