2,3-二甲基马来酸酐合成路线 （共 135 条）
反应条件
in tetrahydrofuran; diethyl ether T=-78°C; 0.5 h; Inert atmosphere;
参考文献
Surmont, Riccardo; Verniest, Guido; De Kimpe, Norbert
Journal of Organic Chemistry, 2010 , vol. 75, # 16 p. 5750 - 5753
反应条件
in diethyl ether T=0°C; 0.5 h; Inert atmosphere;
参考文献
Surmont, Riccardo; Verniest, Guido; De Kimpe, Norbert
Journal of Organic Chemistry, 2010 , vol. 75, # 16 p. 5750 - 5753
反应条件
1: With sodium hydroxide T=185°C; 66 h; 2: With acetyl chloride 2 h; Heating;
参考文献
Carman; Derbyshire; Hansford; Kadirvelraj; Robinson
Australian Journal of Chemistry, 2001 , vol. 54, # 2 p. 117 - 126
反应条件
benzophenone in toluene 168 h; Irradiation;
参考文献
Winzenburg, M.L.; Fields, E.K.; Sinclair, D.P.; Ray, G.J.; Wright, M.E.; Hall, H.K.
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2624 - 2629
反应条件
1: in toluene
T=20°C; 0.25 h;
2: With sodium methylate in methanol
T=20°C; 20 h; Reflux;
3: With hydrogenchloride in ethanol; water
参考文献
Chen, Yuan-Siao; Yu, Hui-Ming; Shie, Jiun-Jie; Cheng, Ting-Jen Rachel; Wu, Chung-Yi; Fang, Jim-Min; Wong, Chi-Huey
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 5 p. 1766 - 1772
反应条件
methanol; 1,1,1,3,3,3-hexamethyl-disilazane in N,N-dimethyl-formamide
16 h; Ambient temperature;
参考文献
Davis; Bit
Tetrahedron Letters, 1990 , vol. 31, # 36 p. 5201 - 5204
反应条件
1: 60 percent / NBS, benzoyl peroxide / CCl4 / 10 h / Heating
2: CuI / diethyl ether; hexamethylphosphoric acid triamide / 8 h / -5 - 20 °C
View Scheme
参考文献
Deshpande, Anil M.; Natu, Arvind A.; Argade, Narshinha P.
Journal of Organic Chemistry, 1998 , vol. 63, # 25 p. 9557 - 9558
反应条件
in toluene
3 h; Heating;
参考文献
Padwa, Albert; Jacquez, Martin N.; Schmidt, Andreas
Journal of Organic Chemistry, 2004 , vol. 69, # 1 p. 33 - 45
反应条件
1: 94 percent / toluene / 3 h / Heating
2: 73 percent / Lawesson's reagent / toluene / 2 h / Heating
View Scheme
参考文献
Padwa, Albert; Jacquez, Martin N.; Schmidt, Andreas
Journal of Organic Chemistry, 2004 , vol. 69, # 1 p. 33 - 45
反应条件
23 in toluene
3 h; Heating;
参考文献
Padwa, Albert; Jacquez, Martin N.; Schmidt, Andreas
Journal of Organic Chemistry, 2004 , vol. 69, # 1 p. 33 - 45
