sodium dithionite; sodium hydrogencarbonate in water; N,N-dimethyl-formamide
T=120°C; 1.5 h; Heating; Yields of byproduct given. Title compound not separated from byproducts;
1: in n-heptane; o-xylene
T=30°C; 1 h;
2: in n-heptane; o-xylene
T=3 - 8°C; 23.6667 h; Product distribution / selectivity;
参考文献
De Boer, Eric Johannes Maria; Van Der Heijden, Harry; Oosterveld, Inge; Van Zon, Arie
Patent: US2006/14989 A1, 2006 ;
Location in patent: Page/Page column 13 ;
[MoO2{(tBuCO)2CH}2] in toluene
T=150°C; 24 h; Autoclave; Reagent/catalyst;
参考文献
Korstanje, Ties J.; Folkertsma, Emma; Lutz, Martin; Jastrzebski, Johann T.B.H.; Klein Gebbink, Robertus J.M.
European Journal of Inorganic Chemistry, 2013 , # 12 p. 2195 - 2204
