反式-2-(4-氨基环己基)乙酸盐酸盐合成路线 (共 4 条)
反应条件
hydrogenchloride 4 h; Heating / reflux;
参考文献
Gobbi, Luca; Jaeschke, Georg; Rodriguez Sarmiento, Rosa Maria; Steward, Lucinda
Patent: US2009/42943 A1, 2009 ;
Location in patent: Page/Page column 10 ;
US 20090042943 A1
反应条件
hydrogenchloride in water
pH=5;
参考文献
Gobbi, Luca; Jaeschke, Georg; Rodriguez Sarmiento, Rosa Maria; Steward, Lucinda
Patent: US2009/42943 A1, 2009 ;
Location in patent: Page/Page column 10 ;
US 20090042943 A1
反应条件
hydrogenchloride; sodium hydroxide; hydrogen; nickel
1.) 130 deg C, 150 atm, 6 h;
参考文献
Karpavichyus, K. I.; Palaima, A. I.; Knunyants, I. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, p. 1689 - 1694
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 10 p. 2374 - 2379
反应条件
hydrogenchloride; sodium hydroxide; hydrogen; nickel
1.) H2O, 130 deg C, 150 atm, 8 h; Yield given. Yields of byproduct given;
参考文献
Karpavichyus, K. I.; Palaima, A. I.; Knunyants, I. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, p. 1689 - 1694
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 10 p. 2374 - 2379