1-溴-3-(溴甲基)-5-氯苯合成路线 （共 3 条）
反应条件
in ethanol Heating / reflux;
参考文献
Plexxikon Inc
Patent: US2008/221127 A1, 2008 ;
Location in patent: Page/Page column 66; 67 ;
反应条件
N-bromosuccinmide; triphenylphosphine in tetrahydrofuran
T=0 - 20°C; 3 h;
参考文献
Bristol-Myers Squibb Company
Patent: US2009/124613 A1, 2009 ;
Location in patent: Page/Page column 27 ;
US 20090124613 A1
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane
T=80°C; 3 h;
参考文献
Gerritz, Samuel; Shi, Shuhao; Zhu, Shirong
Patent: US2006/287287 A1, 2006 ;
Location in patent: Page/Page column 18-19 ;
US 20060287287 A1
