2-炔丙基-N-丁基氨基甲酸酯合成路线 （共 7 条）
反应条件
tetrabutylammomium bromide in acetonitrile
反应条件
in dichloromethane T=40°C; 24 h;
参考文献
Synlett, , # 6 p. 809 - 812
反应条件
sodium hydrogencarbonate in dichloromethane
参考文献
Tetrahedron, , vol. 63, # 37 p. 9153 - 9162
反应条件
triethylamine in toluene 12 h; Reflux;
参考文献
Synthesis, , # 18 art. no. Z09808SS, p. 2919 - 2924
反应条件
1: Methyl N-n-butylthiocarbamate With pyridine; bis(trichloromethyl) carbonate in dichloromethane T=-10°C; 2: propargyl alcohol in dichloromethane T=-10 - 30°C; 14 h;
参考文献
Synthetic Communications, , vol. 34, # 1 p. 33 - 39
反应条件
in tetrachloromethane T=70°C; 3 h;
参考文献
Synthesis, , # 10 art. no. Z03508SS, p. 1612 - 1618
反应条件
1: With sodium hydroxide; sodium hypochlorite; sodium iodide in water T=0 - 40°C; 1.5 h; 2: With acetic acid in water T=40°C; pH=6.9; 3: With sodium hydrogensulfite in water T=25 - 59°C; pH=6.6; Product distribution / selectivity;
参考文献
Schneider, David J.; Schneider, Charles A.; Jones, Kurt A.; Heineke, Martin S.
Patent: US2005/33083 A1, 2005 ;
Location in patent: Page/Page column 3-4 ;
