2,2-二乙氧基乙基磷酸二乙酯合成路线 (共 16 条)
参考文献
Collignon, N.; Fabre, G.; Varlet, J. M.; Savignac, Ph.
Phosphorus and Sulfur and the Related Elements, 1981 , vol. 10, p. 81 - 86
反应条件
1) 142-145 deg C, 4h, 2) 165-168 deg C, 1h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 37, p. 1377 - 1384
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1210 - 1213
反应条件
hydrogenchloride; hydroxylamine hydrochloride Yield given. Multistep reaction;
参考文献
Lee, Kyung Seok; Kang, Yong Koo; Yoo, Kyung Ho; Kim, Dong Chan; Shin, Kye Jung; Paik, Young-Sook; Kim, Dong Jin
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 1 p. 231 - 234
反应条件
1: 33.91 g / 2percent aq. HCl / Heating 2: 48.52 percent / methanol / 0.17 h / 20 °C View Scheme
参考文献
Friese, Anke; Hell-Momeni, Katja; Zuendorf, Ilse; Winckler, Thomas; Dingermann, Theodor; Dannhardt, Gerd
Journal of Medicinal Chemistry, 2002 , vol. 45, # 7 p. 1535 - 1542
反应条件
oxygen T=155 - 163°C;
参考文献
Razumov,A.I. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1969 , vol. 39, p. 392 - 396,369 - 372
反应条件
1: ion-exchange resin <H+ form> 2: NEt3 3: 1 h / 130 °C 4: NaNH2 / liquid ammonia / 2 h / -35 °C 5: H2 / Raney-Ni / ethanol / 70 °C View Scheme
参考文献
Tavs,P.
Chemische Berichte, 1967 , vol. 100, p. 1571 - 1574
反应条件
hydrogenchloride in water Inert atmosphere;
参考文献
Zingle, Catherine; Kuntz, Lionel; Tritsch, Denis; Grosdemange-Billiard, Catherine; Rohmer, Michel
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 21 p. 6563 - 6567,5
Title/Abstract Full Text Show Details
Zingle, Catherine; Kuntz, Lionel; Tritsch, Denis; Grosdemange-Billiard, Catherine; Rohmer, Michel
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 21 p. 6563 - 6567
反应条件
butan-1-ol; deprotonated form; water; hydrogen cation; butan-1-ol Multistep reaction;
参考文献
Sturz, G.; Clement, J. C.; Daniel, A.; Molinier, J.; Lenzi, M.
Bulletin de la Societe Chimique de France, 1981 , vol. 1, # 5-6 p. 161 - 172
反应条件
water; hydrogen cation; butan-1-ol Multistep reaction;
参考文献
Sturz, G.; Clement, J. C.; Daniel, A.; Molinier, J.; Lenzi, M.
Bulletin de la Societe Chimique de France, 1981 , vol. 1, # 5-6 p. 161 - 172