反应条件
1: 1.) tetramethylpiperidine, n-BuLi / 1.) ether, hexane, 0 deg C, 3 h 2: lithium tetramethylpiperidine (LTMP) / diethyl ether; hexane / 24 h 3: 1.) CF3COOH, 2.) LiAlH4 / 1.) benzene, 3 h, 2.) THF, RT, 2 h View Scheme
参考文献
Netka, Jill; Crump, Stephen L.; Rickborn, Bruce
Journal of Organic Chemistry, 1986 , vol. 51, # 8 p. 1189 - 1199