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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
75366-05-1
合成路线
（共 8 条）
75366-05-1
→
反应条件
27561-50-8
1-溴-2-(溴甲基)-4-甲基苯
+
75366-14-2
2-溴-1-(溴甲基)-4-甲基苯
反应条件
bromine in tetrachloromethane T=-10°C; 0.5 h; reaction regioselectivity; a series of reagents; Product distributionMechanism;
参考文献
Bee, Lim Keow; Garratt, Peter J.; Mansuri, Muzamil M.
Journal of the American Chemical Society, 1980 , vol. 102, # 23 p. 7076 - 7079
75366-05-1
→
反应条件
553-94-6
2,5-二甲基溴苯
+
583-70-0
2,4-二甲基溴苯
反应条件
bromine; tri-n-butyl-tin hydride multistep reaction; reaction regioselectivity; a series of reagents; Product distributionMechanism;
参考文献
Bee, Lim Keow; Garratt, Peter J.; Mansuri, Muzamil M.
Journal of the American Chemical Society, 1980 , vol. 102, # 23 p. 7076 - 7079
75366-05-1
→
反应条件
553-94-6
2,5-二甲基溴苯
+
583-70-0
2,4-二甲基溴苯
反应条件
bromine; tri-n-butyl-tin hydride multistep reaction; reaction regioselectivity; a series of reagents; Product distributionMechanism;
参考文献
Bee, Lim Keow; Garratt, Peter J.; Mansuri, Muzamil M.
Journal of the American Chemical Society, 1980 , vol. 102, # 23 p. 7076 - 7079
75366-05-1
→
反应条件
620-19-9
3-甲基苄基氯
+
104-82-5
4-甲基氯苄
反应条件
hydrogenchloride in tetrachloromethane 1 h; Yield given. Yields of byproduct given;
参考文献
Bee, Lim Keow; Garratt, Peter J.; Mansuri, Muzamil M.
Journal of the American Chemical Society, 1980 , vol. 102, # 23 p. 7076 - 7079
75366-05-1
→
反应条件
620-19-9
3-甲基苄基氯
+
104-82-5
4-甲基氯苄
反应条件
hydrogenchloride in tetrachloromethane 1 h; Yield given. Yields of byproduct given;
参考文献
Bee, Lim Keow; Garratt, Peter J.; Mansuri, Muzamil M.
Journal of the American Chemical Society, 1980 , vol. 102, # 23 p. 7076 - 7079
75366-05-1
+
74497-02-2
→
反应条件
15818-64-1
+
75366-13-1
反应条件
silver nitrate in tetrachloromethane 0.5 h; Yield given. Yields of byproduct given;
参考文献
Bee, Lim Keow; Garratt, Peter J.; Mansuri, Muzamil M.
Journal of the American Chemical Society, 1980 , vol. 102, # 23 p. 7076 - 7079
75366-05-1
→
反应条件
27561-50-8
1-溴-2-(溴甲基)-4-甲基苯
+
75366-14-2
2-溴-1-(溴甲基)-4-甲基苯
反应条件
bromine in tetrachloromethane T=-10°C; 0.5 h; reaction regioselectivity; a series of reagents; Product distributionMechanism;
参考文献
Bee, Lim Keow; Garratt, Peter J.; Mansuri, Muzamil M.
Journal of the American Chemical Society, 1980 , vol. 102, # 23 p. 7076 - 7079
64-17-5
乙醇
+
75366-05-1
→
反应条件
64988-09-6
+
54191-22-9
反应条件
silver nitrate in tetrachloromethane 0.5 h; Yield given. Yields of byproduct given;
参考文献
Bee, Lim Keow; Garratt, Peter J.; Mansuri, Muzamil M.
Journal of the American Chemical Society, 1980 , vol. 102, # 23 p. 7076 - 7079
