4,5-二氯-1,2,3-二噻唑氯化物合成路线 （共 32 条）
反应条件
disulfur dichloride in dichloromethane 16 h;
参考文献
SIRTRIS PHARMACEUTICALS, INC.
Patent: WO2009/14674 A1, 2009 ;
Location in patent: Page/Page column 82 ;
WO 2009/014674 A1
参考文献
Hedou, Damien; Guillon, Remi; Lecointe, Charlotte; Loge, Cedric; Chosson, Elizabeth; Besson, Thierry
Tetrahedron, 2013 , vol. 69, # 15 p. 3182 - 3191
反应条件
disulfur dichloride in dichloromethane T=20°C; 12 h;
参考文献
Koutentis, Panayiotis A.
Molecules, 2005 , vol. 10, # 2 p. 346 - 359
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 23, p. 277 - 296
反应条件
water in acetonitrile T=20°C; 6 h;
参考文献
Tetrahedron, , vol. 65, # 34 p. 6855 - 6858
反应条件
in acetonitrile T=20°C; 1 h;
参考文献
Tetrahedron, , vol. 65, # 34 p. 6855 - 6858
反应条件
in liquid sulphur dioxide byproducts: (C2NS2Cl)2; vac.; -70°C, stirring, warming to room temp. (2 h);
参考文献
Barclay; Beer; Cordes; Haddon; Itkis; Oakley; Preuss; Reed
Journal of the American Chemical Society, 1999 , vol. 121, # 28 p. 6657 - 6663
反应条件
pyridine T=20°C; 24 h; Inert atmosphere;
参考文献
Xie, Aming; Cao, Meiping; Liu, Yangyang; Feng, Liandong; Hu, Xinyu; Dong, Wei
European Journal of Organic Chemistry, 2014 , vol. 2014, # 2 p. 436 - 441
反应条件
water Multistep reaction;
参考文献
Mayer, Roland
Phosphorus and Sulfur and the Related Elements, 1985 , vol. 23, p. 277 - 296
反应条件
water; triphenylphosphine in dichloromethane
Ambient temperature;
参考文献
Besson, Thierry; Emayan, Kumaraswamy; Rees, Charles W.
Journal of the Chemical Society, Chemical Communications, 1995 , # 14 p. 1419 - 1420
