in tetrahydrofuran To a flask containing anhyd. N-methylmorpholine-N-oxide at 0°C under N2 is added soln. of nitroso compound and Fe(CO)5 in THF over a period of 30 min (30°C), the soln. is stirred an addnl. 5 min.; biphenyl as an internal standard is added, the mixture is subjected to GC anal.;
参考文献
Herndon, James W.; McMullen, Leonard A.
Journal of Organometallic Chemistry, 1989 , vol. 368, p. 83 - 102