2-[(4-硝基苯甲酰基)氨基]乙酸乙酯合成路线 （共 18 条）
反应条件
N-ethyl-N,N-diisopropylamine in acetonitrile Heating / reflux;
参考文献
F2G LTD
Patent: WO2008/62182 A1, 2008 ;
Location in patent: Page/Page column 153 ;
反应条件
copper(l) iodide; calcium carbonate in water; acetonitrile T=40°C; 6 h;
参考文献
Yoo, Woo-Jin; Li, Chao-Jun
Journal of the American Chemical Society, 2006 , vol. 128, # 40 p. 13064 - 13065
反应条件
water; sodium acetate in acetonitrile T=0°C; 1.16667 h; Inert atmosphere;
参考文献
Basavanag, Unnamatla M. V.; Dos Santos, Aurelie; El Kaim, Laurent; Gamez-Montano, Rocio; Grimaud, Laurence
Angewandte Chemie - International Edition, 2013 , vol. 52, # 28 p. 7194 - 7197
Angew. Chem., 2013 , vol. 125, # 28 p. 7335 - 7338,4
反应条件
Tl(NO3)3*3H2O; triethylamine in acetonitrile Ambient temperature1.) 0 deg C, 10 min, 2.) r.t., 2 h;
参考文献
Kocevar, Marijan; Mihorko, Polona; Polanc, Slovenko
Journal of Organic Chemistry, 1995 , vol. 60, # 5 p. 1466 - 1469
反应条件
sodium hydride in tetrahydrofuran 1.) 0 deg C, 0.5 h; 2.) r.t., 12 h;
参考文献
Rao, M. Narayana; Holkar, A. G.; Ayyangar, N. R.
Tetrahedron Letters, 1989 , vol. 30, # 35 p. 4717 - 4720
反应条件
tert.-butylhydroperoxide; copper(l) iodide; silver(I) iodate; calcium carbonate in water; acetonitrile T=40°C; 6 h;
参考文献
Giguere-Bisson, Maxime; Yoo, Woo-Jin; Li, Chao-Jun
Organic Syntheses, 2012 , vol. 88, p. 14 - 21
参考文献
Journal of Experimental Medicine, , vol. 69, p. 705,707
反应条件
1: SOCl2, DMF / toluene / 0.5 h / 60 - 70 °C 2: K2CO3 / H2O; toluene / -5 - 5 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 28, # 7 p. 2045 - 2051
反应条件
1: 40 percent / lead tetra-acetate / CH2Cl2; acetic acid / 0.5 h / 0 °C 2: triethylamine / dioxane / 4 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 619 - 621
反应条件
1: methanol / Ambient temperature 2: 40 percent / lead tetra-acetate / CH2Cl2; acetic acid / 0.5 h / 0 °C 3: triethylamine / dioxane / 4 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 619 - 621
