Tsoi, E. V.; Afanas'eva, G. B.; Chupakhin, O. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 3 p. 350 - 351
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 3 p. 422
Afanas'eva, G. B.; Tsoi, E. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1991 , vol. 27, # 6 p. 616 - 620
Khimiya Geterotsiklicheskikh Soedinenii, 1991 , vol. 27, # 6 p. 786 - 790
1: 1.) 1,2-dibromoethane, magnesium / 1.) benzene, THF, 2.) -45 deg C -> room temperature, 15 min
2: air / chromatography on SiO2
3: 312 mg / CHCl3 / 144 h / Ambient temperature
View Scheme
参考文献
Forrester, Alexander R.; Fullerton, Joseph D.; McConnachie, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1759 - 1764
1: air / chromatography on SiO2
2: 312 mg / CHCl3 / 144 h / Ambient temperature
View Scheme
参考文献
Forrester, Alexander R.; Fullerton, Joseph D.; McConnachie, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1759 - 1764
1: 1.) 1,2-dibromoethane, magnesium / 1.) benzene, THF, 2.) -45 deg C -> room temperature, 15 min
2: air / chromatography on SiO2
3: 312 mg / CHCl3 / 144 h / Ambient temperature
View Scheme
参考文献
Forrester, Alexander R.; Fullerton, Joseph D.; McConnachie, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1759 - 1764
potassium dihydrogenphosphate; Fremy’s salt in water; acetone
参考文献
Forrester, Alexander R.; Fullerton, Joseph D.; McConnachie, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2711 - 2715
1: 43 mg / CHCl3 / 144 h / Ambient temperature
2: p-t-butylphenyl 4-t-butyl-1-naphthyl nitroxide / CHCl3 / 168 h / other reagent (p-t-butylphenyl 3,7-di-t-butyl-1-naphthyl nitroxide)
View Scheme
参考文献
Forrester, Alexander R.; Fullerton, Joseph D.; McConnachie, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1759 - 1764
