3-(3-甲氧基苯甲酰基)苯甲腈合成路线 （共 6 条）
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tetraethylammonium cyanide; tris(dibenzylideneacetone)dipalladium (0) in 1,4-dioxane 4.5 h; Heating;
参考文献
Inamoto, Kiyofumi; Saito, Tadataka; Katsuno, Mika; Sakamoto, Takao; Hiroya, Kou
Organic Letters, 2007 , vol. 9, # 15 p. 2931 - 2934
反应条件
n-butyllithium in tetrahydrofuran; hexane Inert atmosphere;
参考文献
Hayashi, Yoshio; Yamazaki, Yuri; Sumikura, Makiko; Masuda, Yurika; Hayashi, Yoshiki; Yasui, Hiroyuki; Kiso, Yoshiaki; Chinen, Takumi; Usui, Takeo; Yakushiji, Fumika; Potts, Barbara; Neuteboom, Saskia; Palladino, Michael; Lloyd, George Kenneth
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 14 p. 4279 - 4289
反应条件
1: 100 percent / tetrahydrofuran / 0.25 h / 20 °C 2: 86 percent / MnO2 / CH2Cl2 / 1 h / 20 °C 3: 98 percent / dppf; Et4NCN / Pd2(dba)3 / dioxane / 4.5 h / Heating View Scheme
参考文献
Organic Letters, , vol. 9, # 15 p. 2931 - 2934
反应条件
1: 100 percent / tetrahydrofuran / 0.25 h / 20 °C 2: 86 percent / MnO2 / CH2Cl2 / 1 h / 20 °C 3: 98 percent / dppf; Et4NCN / Pd2(dba)3 / dioxane / 4.5 h / Heating View Scheme
参考文献
Organic Letters, , vol. 9, # 15 p. 2931 - 2934
反应条件
1: 86 percent / MnO2 / CH2Cl2 / 1 h / 20 °C 2: 98 percent / dppf; Et4NCN / Pd2(dba)3 / dioxane / 4.5 h / Heating View Scheme
参考文献
Organic Letters, , vol. 9, # 15 p. 2931 - 2934
反应条件
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C 2: n-butyllithium / tetrahydrofuran; hexane / Inert atmosphere View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 14 p. 4279 - 4289
