in acetone high yield of mesityl oxide by react. with boiling pure acetone; success of reaction depends on the purity of acetone;; impurities of commercial acetone retard or inhibit the reaction;;
参考文献
Bodroux, F.; Taboury, F.
Bulletin de la Societe Chimique de France, 1908 , vol. 3, p. 829 - 833
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Gmelin Handbook: Ca: MVol.B3, 89, page 845 - 848
in neat (no solvent) passing of a mixture of Br2 and air over CaC2 forms CaBr2 at heating;;
参考文献
Barnes, E.
Chem. News J. Ind. Sci., 1919 , vol. 119, p. 260 - 261
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Pope, W. J.
Journal of the Society of Chemical Industry, London, 1923 , vol. 42, p. 117 - 120
West, F. B.; Montonna, R. E.
Journal of Physical Chemistry, 1941 , vol. 45, p. 1179 - 1194
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Gmelin Handbook: Ca: MVol.B3, 86, page 840 - 841
Bobrownicki, W.
Przemysl chem. (poln.), 1924 , vol. 8, p. 7 - 14
C. II, 1924 , p. 1740
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Gmelin Handbook: Ca: MVol.B1, 81, page 182 - 183
in N,N-dimethyl-formamide Sonication; glove box under N2; mixed, ultrasonication at 25+/-5°C for 120h; centrifuged, washed (pentane or hexane), extd. (three times with pentane or hexane), evapd., distn.;
参考文献
Cochran, John C.; Lemieux, Robert P.; Giacobbe, Robert C.; Roitstein, Alexander
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1990 , vol. 20, p. 251 - 262
in N,N-dimethyl-formamide Sonication; glove box under N2; mixed, ultrasonication at 25+/-5°C for 120h; centrifuged, washed (pentane or hexane), extd. (three times with pentane or hexane), evapd., distn.; elem. anal.;
参考文献
Cochran, John C.; Lemieux, Robert P.; Giacobbe, Robert C.; Roitstein, Alexander
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1990 , vol. 20, p. 251 - 262
