2-氯-10H-吖啶-9-酮合成路线 (共 17 条)
参考文献
Nadaraj; Kalaivani; Selvi, S. Thamarai
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 8 p. 1958 - 1960
反应条件
copper(l) iodide in dimethyl sulfoxide; chlorobenzene T=140°C; P=760.051 Torr; 48 h; Schlenk technique;
参考文献
Zhou, Wang; Yang, Youqing; Liu, Yong; Deng, Guo-Jun
Green Chemistry, 2013 , vol. 15, # 1 p. 76 - 80
反应条件
sodium hydroxide; tetrabutylammomium bromide in tetrahydrofuran T=60°C; 2 h;
参考文献
Synthesis, , # 6 p. 448 - 449
反应条件
copper(l) iodide in dimethyl sulfoxide; chlorobenzene T=140°C; P=760.051 Torr; 48 h; Schlenk technique;
参考文献
Zhou, Wang; Yang, Youqing; Liu, Yong; Deng, Guo-Jun
Green Chemistry, 2013 , vol. 15, # 1 p. 76 - 80
反应条件
sulfuric acid; sodium nitrite in water T=20°C; 20 h;
参考文献
Orlov; Ganzha; Kotov; Sokolov
Russian Journal of Organic Chemistry, 2007 , vol. 43, # 10 p. 1502 - 1507
反应条件
potassium hydroxide in isopropyl alcohol 3 h; Heating;
参考文献
Orlov, Vladimir Yu.; Kotov, Aleksandr D.; Ganzha, Valentin V.; Sokolov, Vitaliy G.
Mendeleev Communications, 2004 , vol. 14, # 1 p. 37 - 38
反应条件
BnNMe3(1+)ICl4(1-) in acetic acid 10 h; Ambient temperature;
参考文献
Vlassa; Silberg; Custelceanu; Culea
Synthetic Communications, 1995 , vol. 25, # 21 p. 3493 - 3501
反应条件
ligroin; sodium hydride in dimethyl sulfoxide 24 h; Ambient temperature;
参考文献
Journal of Pharmaceutical Sciences, , vol. 84, # 2 p. 208 - 211
反应条件
1: copper(I) oxide; copper; potassium carbonate / V methoxymethyl ester / 5 h / 140 °C 2: P2O5; phosphoric acid / 3 h / 100 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 4 p. 701 - 711
反应条件
1: copper(I) oxide; copper; potassium carbonate / V methoxymethyl ester / 5 h / 140 °C 2: P2O5; phosphoric acid / 3 h / 100 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 4 p. 701 - 711