氯-(苯基-三甲基硅烷基甲基亚基)膦合成路线 （共 13 条）
反应条件
1: 57 percent / benzene / 0.08 h / 125 °C 2: 78 percent / neat (no solvent) / 130 °C View Scheme
参考文献
Schnurr, Werner; Regitz, Manfred
Tetrahedron Letters, 1989 , vol. 30, # 30 p. 3951 - 3954
反应条件
in diethyl ether T=0 - 5°C; Irradiation;
参考文献
Maerkl, G.; Troetsch-Schaller, I.; Hoelzl, W.
Tetrahedron Letters, 1988 , vol. 29, # 7 p. 785 - 788
反应条件
1,4-diaza-bicyclo[2.2.2]octane in diethyl ether
12 h; Ambient temperature;
参考文献
Appel, Rolf; Westerhaus, Axel
Angewandte Chemie, 1980 , vol. 92, # 7 p. 578
反应条件
1: 1) Mg, 2) PCl3 / 1) diethylether, 2) ether, ice cooling
2: 54 percent / 1,4-diazabicyclo<2.2.2>octane / diethyl ether / 12 h / Ambient temperature
View Scheme
参考文献
Appel, Rolf; Westerhaus, Axel
Angewandte Chemie, 1980 , vol. 92, # 7 p. 578
反应条件
1,2,2-trichloro-1,1,2-trichloro-ethane
Product distribution;
参考文献
Appel, Rolf; Kuendgen, Ursula; Knoch, Falk
Chemische Berichte, 1985 , vol. 118, # 4 p. 1352 - 1370
反应条件
900 deg C, 50 mTorr; -78 deg C;
参考文献
Laurent, J. C. T. R. Burckett St; Cooper, T. A.; Kroto, H. W.; Nixon, J. F.; Ohashi, O.
Journal of Molecular Structure, 1982 , vol. 79, p. 215 - 220
参考文献
Solouki, Bahman; Bock, Hans; Appel, Rolf; Westerhaus, Axel; Becker, Gerd; Uhl, Gudrun
Chemische Berichte, 1982 , vol. 115, # 12 p. 3747 - 3755
反应条件
potassium fluoride; 18-crown-6 ether in xylene
2 h; Heating;
参考文献
Maerkl, Gottfried; Seidl, Ernst; Troetsch, Irene
Angewandte Chemie, 1983 , vol. 95, # 11 p. 891 - 892
反应条件
in diethyl ether
Ambient temperature;
参考文献
Maerkl, Gottfried; Troetsch, Irene
Angewandte Chemie, 1984 , vol. 96, # 11 p. 899 - 901
反应条件
in diethyl ether
Ambient temperature;
参考文献
Maerkl, Gottfried; Troetsch, Irene
Angewandte Chemie, 1984 , vol. 96, # 11 p. 899 - 901
