Talalaeva, T. V.; Kocheshkov, K. A.
Zhurnal Obshchei Khimii, 1938 , vol. 8, p. 1831 - 1838
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Gmelin Handbook: Bi: Org.Verb., 1.3.3.2.4.3, page 72 - 78
in pentane byproducts: NaCl; Inert atm.; a suspn. of BiCl3 in pentane was added to a soln. of cyclophosphane in pentane at room temp.; ppt. was filtered;
in hydrogenchloride Electrolysis; precipitation of a Bi layer on Fe; 70-100 g NaBiCl4 (electrolyte) and 200-300 ml concentrated HCl/l with addition of a small amount of glue, 2-2.7 A/dm*dm;;
in toluene 24 h, vacuum; pptn. of Bi, chromy. (W-complex);
参考文献
Sharutin, V. V.
Journal of General Chemistry USSR (English Translation), 1988 , vol. 58, p. 2050 - 2056
Zhurnal Obshchei Khimii, 1988 , vol. 58, p. 2305 - 2311
