反应条件
in pentane; benzene byproducts: NaCl, LiCl; stirring carborane and NaH (excess, C6H6:TMEDA 1:1, room temp., 6 h), purification of intermediate (Organometallics 1993, 12, 3001), dissoln. (C6H6:TMEDA), addn. of t-BuLi (pentane, 0°C), warming to room temp., addn. to GaCl3 (C6H6, 0°C); stirring at room temp. overnight, filtration off of byproducts, evapn., addn. of C6H6, stirring for 2 h, standing overnight, filtration, concn.;elem. anal.;
参考文献
Organometallics, , vol. 16, # 24 p. 5163 - 5170
