{(C6H5)I}2SbCl5 in acetone
at several temps. and mole ratios;
参考文献
Ptytsyna, O. A.; Reutov, O. A.; Ertel, G.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1961 , p. 241 - 245
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1961 , p. 265 - 270
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Gmelin Handbook: Sb: Org.Comp.2, 1.2.1.1.10.1, page 35 - 38
in neat (no solvent)
formation on heating in an autoclave to 170-280°C;;
参考文献
Emeleus, H. J.
Fortschr. Chem. Forsch., 1951 , vol. 2, p. 609 - 618
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Emeleus, H. J.
Suomen Kemistilehti B, 1958 , vol. 31, p. 101 - 109
in neat (no solvent)
byproducts: C2F4, C3F6, SiF4; carried out under inert atm.; combined and heated to 170°C, detected after 3h to 80h, no longer detected after further 72h at 170°C; not isolated, monitored by NMR;
参考文献
Ganja, E. A.; Morrison, J. A.
Inorganic Chemistry, 1990 , vol. 29, p. 33 - 38
165-170°C (6 h); in autoclave; distn.; (CF3)2SbI contains SbI3;
参考文献
Dale, J. V.; Emeleus, H. J.; Haszeldine, R. N.; Moss, J. H.
Journal of the Chemical Society, 1957 , p. 3708 - 3713
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Gmelin Handbook: F: PerFHalOrg.3, 3, page 226 - 232
lithium in ammonia
ratio of Li (Na), Sb and EtBr 2:1:2;
参考文献
Bogolyubov, G. M.; Shlyk, Yu, N.; Petrov, A. A.
Zhurnal Obshchei Khimii, 1969 , vol. 39, p. 1768 - 1771
Zhurnal Obshchei Khimii, 1969 , vol. 39, p. 1804 - 1808
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Gmelin Handbook: Sb: Org.Comp.2, 1.2.2.1.1, page 74 - 77
