N,N-dimethyl-formamide in neat (no solvent) Sb and I2C6Cl4 heated in sealed tube to 250°C for 4 h; extd. with boiling DMF, extd. with boiling C6H5NO2; elem. anal.;
参考文献
Al-Jabar, N.A.A.; Massey, A.G.
Journal of Organometallic Chemistry, 1984 , vol. 276, # 3 p. 331 - 340
Popolitov, V. I.; Plakhov, G. F.
Inorganic Materials (Transl. of Neorg. Mater.), 1988 , vol. 24, p. 1016 - 1019
Izvestiya Akademii Nauk SSSR, Neorganicheskie Materialy, 1988 , vol. 24, p. 1192 - 1195
in neat (no solvent) Sb and I2C6Cl4 heated in sealed tube to 250°C for 4 h; extd. with boiling DMF, concd., washed (acetone), dried (vac.) at room temp. for 1 h; elem. anal.;
参考文献
Al-Jabar, N.A.A.; Massey, A.G.
Journal of Organometallic Chemistry, 1984 , vol. 276, # 3 p. 331 - 340
165-170°C (6 h); in autoclave; distn.; (CF3)2SbI contains SbI3;
参考文献
Dale, J. V.; Emeleus, H. J.; Haszeldine, R. N.; Moss, J. H.
Journal of the Chemical Society, 1957 , p. 3708 - 3713
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Gmelin Handbook: F: PerFHalOrg.3, 3, page 226 - 232
n-propylamine in water High Pressure; solvatothermal synthesis in Teflon-lined stainless-steel autoclave; Te (99.999 percent), Sb (99.999 percent), 50 wt. percent aq. RbOH (99.9 percent), n-PrNH2 (98 percent), H20 (Te/Sb/Rb2O/n-PrNH2/H2O = 1:0.682:0.774:0.68:19.53 mol) shaked for 1 min and heated at 453 K for 7 ds; quenched in air at ambient temp.; filtered; washed (EtOH); dried in air;manually sepd.; XRD;
参考文献
Shulman, Alexander; Palmqvist, Anders E. C.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 5 p. 718 - 722
Gospodinov, G. G.; Gospodinova, D. B.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1977 , vol. 22, p. 1839 - 1840
Zhurnal Neorganicheskoi Khimii, 1977 , vol. 22, p. 3366 - 3368
