in neat (no solvent, solid phase) metals and Cl2 (arranged in sealed quartz capillary) heated in quartz ampoule from room temp. to 1270 K within 4 h, allowed to stand at this temp. then cooled to room temp. within 1 d;
参考文献
Hampel, Silke; Ruck, Michael
Zeitschrift fur Anorganische und Allgemeine Chemie, 2006 , vol. 632, # 7 p. 1150 - 1156