diethyl N,N-diethylphosphoramidite; sodium perchlorate; sodium salt of phosphorous acid; sodium iodide
1.) acetonitrile, 1.31 Ah of electricity at a current density 1 - 4 mA/cm2, 2.) acetonitrile, reflux, 2h.; Yield given. Multistep reaction;
参考文献
Romakhin; Zagumennov; Nikitin
Russian Journal of General Chemistry, 1997 , vol. 67, # 4 p. 563 - 566