4-甲基-4-苯基-2-戊酮合成路线 （共 43 条）
反应条件
potassium hydroxide; hydrazine hydrate; diethylene glycol
T=200°C;
参考文献
Hughes
Journal of the Chemical Society, 1958 , p. 3703,3705
参考文献
Gelin,R.; Chantegrel,B.
Bulletin de la Societe Chimique de France, 1971 , p. 2527 - 2544
参考文献
Hoffman
Journal of the American Chemical Society, 1929 , vol. 51, p. 2545
反应条件
1: Br2, alkaline
2: 1.) PCl5, 2.) AlCl3 / 1) C6H6
3: KNO3, H2SO4 / 0 °C
4: 1.) H2, 2.) NaNO2, HCl, 3.) H2SO4, H2O / 1.) PtO / 2) 0 deg C; 3) heating
5: K2CO3 / acetone
View Scheme
参考文献
Bott, Garry; Field, Leslie D.; Sternhell, Sever
Journal of the American Chemical Society, 1980 , vol. 102, # 17 p. 5618 - 5626
反应条件
disodium hydrogenphosphate; dichloromethane
参考文献
Wilt; Danielzadeh
Journal of Organic Chemistry, 1958 , vol. 23, p. 920
反应条件
toluene-4-sulfonic acid; benzene
Unter Entfernen des entstehenden Wassers;
参考文献
Bergmann et al.
Recueil des Travaux Chimiques des Pays-Bas, 1952 , vol. 71, p. 213,222
反应条件
1: diethyl ether
2: aqueous H2SO4
View Scheme
参考文献
Bogert; Davidson
Journal of the American Chemical Society, 1934 , vol. 56, p. 185,187
反应条件
2: (i) AcOH, H2SO4, (ii) /BRN= 2089341/
3: aq. NaOH / 170 °C
4: SO2Cl2 / hexane
5: (i) NaOH, benzene, (ii) tBuOCl, hexane
View Scheme
参考文献
Prochazka,M.
Collection of Czechoslovak Chemical Communications, 1976 , vol. 41, p. 1557 - 1564
反应条件
2: (i) AcOH, H2SO4, (ii) /BRN= 2089341/
View Scheme
参考文献
Prochazka,M.
Collection of Czechoslovak Chemical Communications, 1976 , vol. 41, p. 1557 - 1564
反应条件
2: (i) AcOH, H2SO4, (ii) /BRN= 2089341/
3: aq. NaOH / 170 °C
4: SO2Cl2 / hexane
View Scheme
参考文献
Prochazka,M.
Collection of Czechoslovak Chemical Communications, 1976 , vol. 41, p. 1557 - 1564
