9-(三甲基甲硅烷基)芴合成路线 （共 37 条）
反应条件
1: 9H-fluorene With n-butyllithium in diethyl ether; hexane T=-78°C; 2: chloro-trimethyl-silane in diethyl ether; hexane T=-78°C;
参考文献
Silaghi-Dumitrescu, Ioan; Cretiu, Gabriela; Silaghi-Dumitrescu, Luminita; Haiduc, Ionel; Toscano, Alfredo; Cea-Olivares, Raymundo
Revue Roumaine de Chimie, 2001 , vol. 46, # 4 p. 289 - 295
参考文献
Gilman et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 1689
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Gilman, H.; Brook, A. G.; Miller, L. S.
Journal of the American Chemical Society, 1953 , vol. 75, p. 4531 - 4534
反应条件
n-butyllithium; chloro-trimethyl-silane in tetrahydrofuran; hexane; water; pentane
参考文献
US5393911 A1, ;
US5191132 A1, ;
反应条件
n-butyllithium in tetrahydrofuran 2 h; Ambient temperature; Yield given;
参考文献
Journal of Organometallic Chemistry, , vol. 525, # 1-2 p. 15 - 22
反应条件
1,2-benzanthracene in tetrahydrofuran T=25°C; also with 9-benzylbenzo<def>fluorene; Equilibrium constant;
参考文献
Journal of Organic Chemistry, , vol. 58, p. 1778 - 1784
反应条件
9-methyl-9H-fluorene in tetrahydrofuran T=25°C; also with 4,5-methylenephenanthrene; Equilibrium constant;
参考文献
Journal of Organic Chemistry, , vol. 58, p. 1778 - 1784
反应条件
1.) 180 deg C, 72 h, 2.) ether; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 51, # 9 p. 1632 - 1633
参考文献
Journal of the Chemical Society, , p. 1420,1425
反应条件
different active methylene compounds, reagent and reaction times; Product distribution;
参考文献
Recueil: Journal of the Royal Netherlands Chemical Society, , vol. 102, # 9 p. 400 - 404
反应条件
tetrachloromethane; N-bromosuccinmide
参考文献
Zaitseva, Galina S.; Karlov, Sergey S.; Siggelkow, Bettina A.; Avtomonov, Evgeni V.; Churakov, Andrei V.; Howard, Judith A.K.; Lorberth, Joerg
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1998 , vol. 53, # 11 p. 1247 - 1254
