1,2-双(三甲基硅氧基)乙烷合成路线 （共 58 条）
反应条件
bismuth trifluoromethanesulphonate
T=20°C; 4 h;
参考文献
Podgorski, Daniel M.; Krabbe, Scott W.; Le, Long N.; Sierszulski, Paul R.; Mohan, Ram S.
Synthesis, 2010 , # 16 art. no. M01810SS, p. 2771 - 2775
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
T=-78°C; Addition; 1 h;
参考文献
Beddie, David G.; Farnham, Andrew W.; Khambay, Bhupinder P. S.
Pesticide Science, 1995 , vol. 44, # 3 p. 261 - 268
反应条件
Nafion-TMS in chloroform
10 h; Heating;
参考文献
Carlson, Rolf; Gautun, Hanna; Westerlund, Andreas
Advanced Synthesis and Catalysis, 2002 , vol. 344, # 1 p. 57 - 60
反应条件
lithium perchlorate in dichloromethane
0.166667 h; Ambient temperatureelectrolysis (platinum electrodes, 10 V, 0.4-0.5 mA);
参考文献
Torii, Sigeru; Inokuchi, Tsutomu
Chemistry Letters, 1983 , p. 1349 - 1350
反应条件
bismuth trifluoromethanesulphonate
14 h;
参考文献
Podgorski, Daniel M.; Krabbe, Scott W.; Le, Long N.; Sierszulski, Paul R.; Mohan, Ram S.
Synthesis, 2010 , # 16 art. no. M01810SS, p. 2771 - 2775
反应条件
Nafion-TMS
T=90 - 95°C; 5 h;
参考文献
Carlson, Rolf; Gautun, Hanna; Westerlund, Andreas
Advanced Synthesis and Catalysis, 2002 , vol. 344, # 1 p. 57 - 60
反应条件
Nafion-TMS in chloroform
68 h; Heating;
参考文献
Carlson, Rolf; Gautun, Hanna; Westerlund, Andreas
Advanced Synthesis and Catalysis, 2002 , vol. 344, # 1 p. 57 - 60
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
T=-78°C; 20 h;
参考文献
Hwu, Jih Ru; Leu, Lish-Cheng; Robl, Jeffrey A.; Anderson, Denise A.; Wetzel, John M.
Journal of Organic Chemistry, 1987 , vol. 52, # 2 p. 188 - 191
