1: 3-chloro-1-phenylprop-1-ene With (η5-C5Me5)2-(Zr=O)-(4-(3-phenylpropyl)pyridin-1-yl) in benzene
T=45°C; 8 h;
2: t-butyldimethylsiyl triflate in benzene
T=105°C; 14 h; Further stages.;
参考文献
Fox, Richard J.; Lalic, Gojko; Bergman, Robert G.
Journal of the American Chemical Society, 2007 , vol. 129, # 46 p. 14144 - 14145
lt;Ir(cod)2gt;PF6-2Bu3P; hydrogen in dichloromethane; acetone
0.5 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ohmura, Toshimichi; Shirai, Yasuo; Yamamoto, Yasunori; Miyaura, Norio
Chemical Communications, 1998 , # 13 p. 1337 - 1338
