(4-甲酰基苯氧基)乙酸甲酯合成路线 (共 11 条)
反应条件
potassium carbonate in acetone T=60°C; 5 h;
参考文献
Wen, Huan; Zhou, Yayao; Lin, Chonglan; Ge, Hui; Ma, Lin; Wang, Zihou; Peng, Wenlie; Song, Huacan
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 8 p. 2123 - 2125
反应条件
potassium carbonate in acetone T=20°C; 3.5 h;
参考文献
Hoogendoorn, Sascha; Blom, Annet E. M.; Willems, Lianne I.; Van Der Marel, Gijsbert A.; Overkleeft, Herman S.
Organic Letters, 2011 , vol. 13, # 20 p. 5656 - 5659
反应条件
1: 4-hydroxy-benzaldehyde With potassium carbonate; potassium iodide in DMF (N,N-dimethyl-formamide) T=20 - 40°C; 2: bromoacetic acid methyl ester T=40 - 70°C; 4 h;
参考文献
WO2005/12280 A1, ;
Page/Page column 48-49 ;
WO 2005/012280 A1
反应条件
triphenylphosphine in tetrahydrofuran; diethylazodicarboxylate
参考文献
Beecham Group p.l.c.
Patent: US4713486 A1, 1987 ;
参考文献
US2006/281751 A1, ;
Page/Page column 25 ;
US 20060281751 A1
反应条件
1: 70 percent / sodium hydroxide, potassium iodide / H2O / 3 h / Heating 2: sulfuric acid View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 35, # 5 p. 409 - 412
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 35, # 5 p. 409 - 412
参考文献
Russian Journal of Organic Chemistry, , vol. 44, # 5 p. 657 - 670
反应条件
1: aq. KOH / methanol; tetrahydrofuran 2: aq. sodium dodecyl sulfate, HCl / 0.75 h 3: 2,3,5,6-tetrachloro-1,4-benzoquinone / H2O; tetrahydrofuran View Scheme
参考文献
Karmakar, Anirban; Goldberg, Israel
CrystEngComm, 2010 , vol. 12, # 12 p. 4095 - 4100
反应条件
sodium hydroxide in tetrahydrofuran; water 0.5 h;
参考文献
Wen, Huan; Zhou, Yayao; Lin, Chonglan; Ge, Hui; Ma, Lin; Wang, Zihou; Peng, Wenlie; Song, Huacan
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 8 p. 2123 - 2125