2-氯-6-甲氧基喹啉-3-甲醛合成路线 (共 15 条)
反应条件
trichlorophosphate T=85°C; 24 h;
参考文献
Fernandez-Galleguillos, Carlos; Saavedra, Luis A.; Gutierrez, Margarita
Journal of the Brazilian Chemical Society, 2014 , vol. 25, # 2 p. 365 - 371
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in neat (no solvent) T=20°C; 2.5 h; Milling;
参考文献
Achar, Tapas Kumar; Maiti, Saikat; Mal, Prasenjit
RSC Advances, 2014 , vol. 4, # 25 p. 12834 - 12839
反应条件
trichlorophosphate in N-methyl-acetamide; ice-water
反应条件
1: acetic acid / Reflux 2: trichlorophosphate / 70 - 80 °C View Scheme
参考文献
Oriental Journal of Chemistry, , vol. 26, # 4 p. 1257 - 1264
反应条件
phosphorus pentachloride; trichlorophosphate T=100°C; 4 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1520 - 1530
反应条件
trichlorophosphate T=60°C; 16 h;
参考文献
Pawar; Bajare; Mundade
Journal of the Indian Chemical Society, 1990 , vol. 67, # 8 p. 685 - 686
反应条件
1: potassium carbonate / acetone / 12 h / |Reflux; |Inert atmosphere 2: trichlorophosphate / N,N-dimethyl-formamide / 0 - 80 °C / |Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 22 p. 8400 - 8408
参考文献
Heterocycles, , vol. 21, # 2 p. 568
反应条件
sodium tetrahydroborate in methanol T=0°C; 0.5 h;
参考文献
Eisai RandD Management Co., Ltd.
Patent: EP2062901 A1, 2009 ;
Location in patent: Page/Page column 19 ;
反应条件
mesoporous nickel hydroxyapatite nanocomposite Henry reaction; 0.0166667 h; Microwave irradiationNeat (no solvent);
参考文献
Neelakandeswari; Sangami; Emayavaramban; Karvembu; Dharmaraj; Kim, Hak Yong
Tetrahedron Letters, 2012 , vol. 53, # 24 p. 2980 - 2984