4'-硝基对甲苯磺酰苯胺合成路线 （共 34 条）
反应条件
(Na1752K0.144Ca0365Mg0.065)(Al2044Si2774O96)*19.16H2O in ethanol T=25 - 30°C; 2 h; SonicationGreen chemistry;
参考文献
Nasrollahzadeh, Mahmoud; Ehsani, Ali; Rostami-Vartouni, Akbar
Ultrasonics Sonochemistry, 2014 , vol. 21, # 1 p. 275 - 282
反应条件
copper(l) iodide; N-methyl-2-(methylamino)ethylamine in 1,4-dioxane T=100 - 110°C; 6 h; Inert atmosphere;
参考文献
Hosseinzadeh, Rahman; Tajbakhsh, Mahmood; Mohadjerani, Maryam; Alikarami, Mohammad
Journal of Chemical Sciences, 2010 , vol. 122, # 2 p. 143 - 148
反应条件
potassium hydroxide in dimethyl sulfoxide; tert-butyl alcohol T=110°C; 21 h;
参考文献
Jammi, Suribabu; Sakthivel, Sekarpandi; Rout, Laxmidhar; Mukherjee, Tathagata; Mandai, Santu; Mitra, Raja; Saha, Prasenjit; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2009 , vol. 74, # 5 p. 1971 - 1976
反应条件
sodium hydride in N,N-dimethyl-formamide T=20 - 50°C;
参考文献
Bunce, Richard A.; Smith, Christopher L.; Knight, Christopher L.
Organic Preparations and Procedures International, 2004 , vol. 36, # 5 p. 482 - 487
反应条件
copper(l) iodide; 1,10-phenanthroline; Cu; potassium carbonate in N,N-dimethyl-formamide T=110°C; 24 h;
参考文献
Yavari; Solgi; Ghazanfarpour-Darjani; Ahmadian
Journal of the Iranian Chemical Society, 2012 , vol. 9, # 6 p. 977 - 981
反应条件
tert.-butylnitrite in acetonitrile T=45°C; 6 h; SolventTemperatureTimeConcentration;
参考文献
Chemical Communications, , vol. 49, # 5 p. 514 - 516
反应条件
sodium in tetrahydrofuran 72 h; Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 38, # 5 p. 1379 - 1388
反应条件
1: 1.) NEt3 / 1.) THF, 0 deg C, 1 d 2.) THF, reflux, 2.5 h 2: 77 percent / Na / tetrahydrofuran / 72 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 38, # 5 p. 1379 - 1388
反应条件
1: pyridine / 16 h / |Reflux 2: tert.-butylnitrite / acetonitrile / 6 h / 45 °C View Scheme
参考文献
Chemical Communications, , vol. 49, # 5 p. 514 - 516
反应条件
potassium tert-butylate in tetrahydrofuran 24 h; Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 38, # 5 p. 1379 - 1388
