3-甲氧基-4-氨基苯甲酸甲酯合成路线 （共 6 条）
反应条件
palladium 10 on activated carbon; hydrogen in ethanol
P=760.051 Torr; 168 h; Darkness;
参考文献
Bhuiyan, M. Delower H.; Zhu, Kai-Xian; Jensen, Paul; Try, Andrew C.
European Journal of Organic Chemistry, 2010 , # 24 p. 4662 - 4670
反应条件
sulfuric acid
6 h; Heating;
参考文献
Taran; Renard; Bernard; Mioskowski; Frobert; Pradelles; Grassi
Journal of the American Chemical Society, 1998 , vol. 120, # 14 p. 3332 - 3339
反应条件
1: 95.9 percent / conc. H2SO4 / benzene / 24 h / Heating
2: 74.6 percent / H2 / PtO2 / ethanol / 72 h / 3361.5 Torr / Ambient temperature
View Scheme
参考文献
Ismail, Ibrahim A.; Sharp, Dale E.; Chedekel, Miles R.
Journal of Organic Chemistry, 1980 , vol. 45, # 11 p. 2243 - 2246
参考文献
NeoRx Corporation
Patent: US6024937 A1, 2000 ;
反应条件
1: 90 percent / aq. NaOH / H2O / 80 °C
2: 100 percent / KMnO4, Na2CO3 / H2O / 1.5 h / Heating
3: 95.9 percent / conc. H2SO4 / benzene / 24 h / Heating
4: 74.6 percent / H2 / PtO2 / ethanol / 72 h / 3361.5 Torr / Ambient temperature
View Scheme
参考文献
Ismail, Ibrahim A.; Sharp, Dale E.; Chedekel, Miles R.
Journal of Organic Chemistry, 1980 , vol. 45, # 11 p. 2243 - 2246
反应条件
1: 100 percent / KMnO4, Na2CO3 / H2O / 1.5 h / Heating
2: 95.9 percent / conc. H2SO4 / benzene / 24 h / Heating
3: 74.6 percent / H2 / PtO2 / ethanol / 72 h / 3361.5 Torr / Ambient temperature
View Scheme
参考文献
Ismail, Ibrahim A.; Sharp, Dale E.; Chedekel, Miles R.
Journal of Organic Chemistry, 1980 , vol. 45, # 11 p. 2243 - 2246
