1: With n-butyllithium; potassium tert-butylate in tetrahydrofuran; hexane T=0°C; 0.333333 h; 2: With (MeO)2BF in tetrahydrofuran; hexane T=-75°C; 3: With dihydrogen peroxide Alkaline hydrolysis; Title compound not separated from byproducts;
magnesium
T=600°C; P=0.01 - 0.1 Torr; Title compound not separated from byproducts;
参考文献
Aitken, R. Alan; Hodgson, Philip K.G.; Morrison, John J.; Oyewale, Adebayo O.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 3 p. 402 - 415
