3,5-二甲氧基苯甲醛合成路线 （共 226 条）
反应条件
1: 1.) Mg, I2
2: p-TsOH / benzene
3: 89 percent / H2 / 10percent Pd/C
4: BBr3 / CH2Cl2
View Scheme
参考文献
Lytollis, William; Scannell, Ralph T.; An, Haoyun; Murty; Reddy, K. Sambi; Barr, John R.; Hecht, Sidney M.
Journal of the American Chemical Society, 1995 , vol. 117, # 51 p. 12683 - 12690
反应条件
1: 98 percent / diethyl ether / 3 h / 0 °C
2: 62 percent / trifluoroacetic acid; NaBH3CN / CH2Cl2 / 3 h / 0 °C
View Scheme
参考文献
Ikeda, Toshiaki; Lintuluoto, Juha M.; Aratani, Naoki; Zin, Seok Yoon; Kim, Dongho; Osuka, Atsuhiro
European Journal of Organic Chemistry, 2006 , # 14 p. 3193 - 3204
反应条件
diethyl ether; boron trifluoride in dichloromethane
15 h;
参考文献
Qi, Longwu; Yamamoto, Noboru; Meijler, Michael M.; Altobell III, Laurence J.; Koob, George F.; Wirsching, Peter; Janda, Kim D.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 23 p. 7389 - 7399
反应条件
sodium methylate in N,N-dimethyl-formamide
T=20°C; Wittig reaction; 10 h;
参考文献
Cai, Wenqing; Zhang, Liangwei; Song, Yanlin; Zhang, Baoxin; Cui, Xuemei; Hu, Guanming; Fang, Jianguo
Free Radical Research, 2011 , vol. 45, # 11-12 p. 1379 - 1387
反应条件
1: acetic anhydride; triethylamine
2: copper; quinoline
View Scheme
参考文献
Ding, De-Jun; Cao, Xiao-Yan; Dai, Fang; Li, Xiu-Zhuang; Liu, Guo-Yun; Lin, Dong; Fu, Xing; Jin, Xiao-Ling; Zhou, Bo
Food Chemistry, 2012 , vol. 135, # 3 p. 1011 - 1019
反应条件
1: (i) Et2O, (ii) H2, Pd-C, AcOEt
3: K2CO3 / acetone
View Scheme
参考文献
Achenbach; Kohl; Kunze
Chemische Berichte, 1979 , vol. 112, # 5 p. 1841 - 1848
