5,5-二甲己烷2,4-二酮合成路线 (共 27 条)
参考文献
Journal of the American Chemical Society, , vol. 56, p. 2665,2666
反应条件
sulfuric acid in ethanol 2 h; Heating;
参考文献
Sosnovskikh, V. Ya.; Ovsyannikov, I. S.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 10 p. 1801 - 1805
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 10 p. 2086 - 2091
参考文献
Journal of the American Chemical Society, , vol. 67, p. 284
反应条件
1: 89 percent / toluene-4-sulphonic acid / benzene / 24 h / Heating 2: 1.) pyridine, H2SO4, 2.) aq. HCl / 1.) reflux, 2.5 h, 2.) ethanol, reflux, 3 h View Scheme
参考文献
Australian Journal of Chemistry, , vol. 37, # 7 p. 1453 - 1460
反应条件
1: 1.) magnesium ethoxide / toluene / 2 h / Ambient temperature; 1.) 0 - 5 deg C, 1 h 2: p-toluenesulfonic acid / toluene / 3 h / 80 °C View Scheme
参考文献
Farmaco, Edizione Scientifica, , vol. 39, # 6 p. 538 - 558
反应条件
sodium hydride; benzene
参考文献
Journal of Organic Chemistry, , vol. 16, p. 57,58
反应条件
pyridine; hydrogenchloride; sulfuric acid 1.) reflux, 2.5 h, 2.) ethanol, reflux, 3 h; Yield given;
参考文献
Australian Journal of Chemistry, , vol. 37, # 7 p. 1453 - 1460
反应条件
T=24°C; Equilibrium constant;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 46, p. 632 - 634
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 150, p. 928
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 150, p. 928