2-(4-硝基苯基)-1H-苯并咪唑合成路线 （共 52 条）
反应条件
1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 60 °C
2: 2-iodosylbenzoic acid / dimethyl sulfoxide / 9 h / 25 °C
View Scheme
参考文献
Moorthy, Jarugu Narasimha; Neogi, Ishita
Tetrahedron Letters, 2011 , vol. 52, # 30 p. 3868 - 3871
反应条件
1: 1,4-dioxane; water / 6 h / 20 °C / |Inert atmosphere
2: acetic acid / 5 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Chang, Meng-Yang; Chan, Chieh-Kai; Chen, Yi-Chia
Heterocycles, 2014 , vol. 89, # 5 p. 1229 - 1236
反应条件
acetic acid
T=20°C; 5 h; Inert atmosphere;
参考文献
Chang, Meng-Yang; Chan, Chieh-Kai; Chen, Yi-Chia
Heterocycles, 2014 , vol. 89, # 5 p. 1229 - 1236
反应条件
hydrogenchloride in methanol
Heating;
参考文献
Orlov, V. D.; Kolos, N. N.; Zolotarev, B. M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 3 p. 318 - 323
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 3 p. 390 - 396
反应条件
in sulfolane
T=350°C; Yield given. Yields of byproduct given;
参考文献
Ochoa, Carmen; Rodriguez, Juan
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 3 p. 1053 - 1055
反应条件
in various solvent(s)
48 h; Heating;
参考文献
Houghton, Peter G.; Pipe, David F.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1471 - 1480
反应条件
1: water
2: concentrated hydrochloric acid / unter Druck
View Scheme
参考文献
Walther; v. Pulawski
Journal fuer Praktische Chemie (Leipzig), 1899 , vol. <2> 59, p. 261
参考文献
Hinsberg; Funcke
Chemische Berichte, 1894 , vol. 27, p. 2188
参考文献
Kroehnke; Leister
Chemische Berichte, 1958 , vol. 91, p. 1479,1486
反应条件
T=330°C; P=0.045004 Torr; 0.25 h; Product distribution; Further Variations:TemperaturesPressures;
参考文献
Al-Awadi, Nouria A.; George, Bobby J.; Dib, Hicham H.; Ibrahim, Maher R.; Ibrahim, Yehia A.; El-Dusouqui, Osman M. E.
Tetrahedron, 2005 , vol. 61, # 34 p. 8257 - 8263
